• Türkçe
    • English
  • English 
    • Türkçe
    • English
  • Login
View Item 
  •   DSpace@Artvin
  • Fakülteler
  • Eğitim Fakültesi
  • Matemetik ve Fen Bilimleri Eğitimi Bölümü
  • Matematik ve Fen Bilimleri Eğitimi Bölümü Koleksiyonu
  • View Item
  •   DSpace@Artvin
  • Fakülteler
  • Eğitim Fakültesi
  • Matemetik ve Fen Bilimleri Eğitimi Bölümü
  • Matematik ve Fen Bilimleri Eğitimi Bölümü Koleksiyonu
  • View Item
JavaScript is disabled for your browser. Some features of this site may not work without it.

Crystal structure and Hirshfeld surface analysis of 3-(hydroxymethyl)-3-methyl-2,6-diphenylpiperidin-4-one

Thumbnail

View/Open

mustafakemal_gumus.pdf (896.6Kb)

Access

info:eu-repo/semantics/openAccess

Date

2022

Author

Gümüş, Mustafa Kemal
Kansız, Sevgi
Tulemisova, Gulzhamal Bagitovna
Dege, Necmi
Saif, Eiad

Metadata

Show full item record

Citation

Gümüş, M. K., Kansiz, S., Tulemisova, G. B., Dege, N., & Saif, E. (2022). Crystal structure and Hirshfeld surface analysis of 3-(hydroxymethyl)-3-methyl-2, 6-diphenylpiperidin-4-one. Acta Crystallographica Section E: Crystallographic Communications, 78(1), 29-32, 1.

Abstract

A new synthesis of the title compound, C19H21NO2, was developed with good yield and purity using the reaction of 4-hy­droxy-3-methyl-2-butanone, benzaldehyde and ammonium acetate in glacial acetic acid as a solvent. The central piperidine ring adopts a chair conformation, and its least-squares basal plane forms dihedral angles of 85.71 (11) and 77.27 (11)° with the terminal aromatic rings. In the crystal, the mol­ecules are linked by O-H⋯O and C-H⋯O hydrogen bonds into double ribbons. The Hirshfeld surface analysis shows that the most important contributions are from H⋯H (68%), C⋯H/H⋯C (19%) and O⋯H/H⋯O (12%) inter­actions.

Source

Acta Crystallographica Section E: Crystallographic Communications

Volume

78

Issue

1

URI

https://hdl.handle.net/11494/3718

Collections

  • Matematik ve Fen Bilimleri Eğitimi Bölümü Koleksiyonu [107]
  • PubMed İndeksli Yayınlar Koleksiyonu [214]
  • Scopus İndeksli Yayınlar Koleksiyonu [1029]
  • WoS İndeksli Yayınlar Koleksiyonu [1322]



DSpace software copyright © 2002-2015  DuraSpace
Contact Us | Send Feedback
Theme by 
@mire NV
 

 




| Policy | Guide | Contact |
Advanced Search

sherpa/romeo

Browse

All of DSpaceCommunities & CollectionsBy Issue DateAuthorsInstitution AuthorORCIDTitlesSubjectsTypeLanguageDepartmentCategoryPublisherAccess TypeThis CollectionBy Issue DateAuthorsInstitution AuthorORCIDTitlesSubjectsTypeLanguageDepartmentCategoryPublisherAccess Type

My Account

LoginRegister

Statistics

View Google Analytics Statistics

DSpace software copyright © 2002-2015  DuraSpace
Contact Us | Send Feedback
Theme by 
@mire NV
 

 


|| Policy || Guide || Library || Artvin Çoruh University || OAI-PMH ||

Artvin Çoruh University, Artvin, Turkey
If you find any errors in content, please contact:

Creative Commons License
Artvin Çoruh University Institutional Repository is licensed under a Creative Commons Attribution-NonCommercial-NoDerivs 4.0 Unported License..

DSpace@Artvin:


DSpace 6.2

tarafından İdeal DSpace hizmetleri çerçevesinde özelleştirilerek kurulmuştur.