Crystal structure and Hirshfeld surface analysis of 3-(hydroxymethyl)-3-methyl-2,6-diphenylpiperidin-4-one

Basit Öğe Kaydı
dc.authorid0000-0001-6373-5221en_US
dc.contributor.authorGümüş, Mustafa Kemal
dc.contributor.authorKansız, Sevgi
dc.contributor.authorTulemisova, Gulzhamal Bagitovna
dc.contributor.authorDege, Necmi
dc.contributor.authorSaif, Eiad
dc.date.accessioned2022-02-14T08:52:59Z
dc.date.available2022-02-14T08:52:59Z
dc.date.issued2022
dc.departmentAÇÜ, Artvin Meslek Yüksekokulu, Laboratuvar Teknolojisi Bölümüen_US
dc.description.abstractA new synthesis of the title compound, C19H21NO2, was developed with good yield and purity using the reaction of 4-hy­droxy-3-methyl-2-butanone, benzaldehyde and ammonium acetate in glacial acetic acid as a solvent. The central piperidine ring adopts a chair conformation, and its least-squares basal plane forms dihedral angles of 85.71?(11) and 77.27?(11)° with the terminal aromatic rings. In the crystal, the mol­ecules are linked by O-H?O and C-H?O hydrogen bonds into double ribbons. The Hirshfeld surface analysis shows that the most important contributions are from H?H (68%), C?H/H?C (19%) and O?H/H?O (12%) inter­actions.
dc.identifier.citationGümüş, M. K., Kansiz, S., Tulemisova, G. B., Dege, N., & Saif, E. (2022). Crystal structure and Hirshfeld surface analysis of 3-(hydroxymethyl)-3-methyl-2, 6-diphenylpiperidin-4-one. Acta Crystallographica Section E: Crystallographic Communications, 78(1), 29-32, 1.en_US
dc.identifier.doi10.1107/S2056989021012640
dc.identifier.endpage32en_US
dc.identifier.issue1en_US
dc.identifier.scopusqualityQ3
dc.identifier.startpage29en_US
dc.identifier.urihttps://hdl.handle.net/11494/3718
dc.identifier.volume78en_US
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorGümüş, Mustafa Kemal
dc.language.isoenen_US
dc.publisherInternational Union of Crystallographyen_US
dc.relation.ispartofActa Crystallographica Section E: Crystallographic Communications
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subject4-hydroxy-3-methyl-2-butanoneen_US
dc.subjectAmmonium acetateen_US
dc.subjectBenzaldehydeen_US
dc.subjectCrystal structureen_US
dc.subjectHirshfeld surfaceen_US
dc.subjectHydrogen bondingen_US
dc.subjectPiperidoneen_US
dc.titleCrystal structure and Hirshfeld surface analysis of 3-(hydroxymethyl)-3-methyl-2,6-diphenylpiperidin-4-oneen_US
dc.typeArticle

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Küçük Resim
İsim:
mustafakemal_gumus.pdf
Boyut:
896.68 KB
Biçim:
Adobe Portable Document Format
Açıklama:
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

Matematik ve Fen Bilimleri Eğitimi Bölümü Koleksiyonu
PubMed İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu
WoS İndeksli Yayınlar Koleksiyonu